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Methods: Absorbite was used to Absorb MTBE. Sample was desorbed by CS2, separated by FFAP resilience quartz capillary column and detected with mass spectra SIM. 空气中MTBE用活性碳管吸附采集，二硫化碳解吸，FFAP弹性石英毛细管柱分离，质谱SIM方式检测。